Perbandingan Metode Microwave Assisted Distillation (MAD) dan Microwave Assisted Hydro Distillation (MAHD) terhadap Jumlah Yield dan Mutu Minyak Atsiri dari Kulit Jeruk Manis (Citrus Aurantium)
Abstract
Kata kunci : minyak atsiri; microwave; kulit jeruk manis; ekstraksi
ABSTRACT
This orange peel extraction was conducted with the aim of knowing and comparing the yield and quality data of citrus peel oil by comparing microwave assisted distillation (MAD) and microwave assisted hydrodistillation (MAHD) methods, and for knowing chemical compounds obtained by GC test -MS. Operating condition is 75 minutes with temperature 100O C with 100 watt microwave power, solvent volume method MAHD is 200 liter. The result of this research was obtained rendemen on MAHD method 2,9ml / 400gram, while MAD method equal to 2,7ml / 400gram. The chemical composition of the sweet orange peel oil obtained from the MAD and MAHD methods is generally the same limonen (C10H16) and linalool (C10H18O). The result of MAD method obtained the amount of oxygenated compounds (3,14%), MAHD method (0,63%). While the amount of non-oxygenated compounds for MAD method (97.97%), MAHD method (99.37%).
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Adrian, P. 2000. Analisa Ekstraktif Tumbuhan sebagai Sumber Bahan Obat. Pusat Penelitian. Universitas Negeri Andalas.
Cahyono, B. 2005. Budidaya Jeruk Mandarin. Yayasan Pustaka Nusantara. Yogyakarta.
Capson, D. A. (1975). Microwave Heating Connecticut : The AVI Publishing Company.Taylor,M. (2005). Developmentsin Microwave Chemistry.Evalueserve.
Calinescu, I., Ciuculescu, C,. Popescu, M. Bejanaru, S., & Epure, G. (2001). Microwaves Assisted Extraction of Active Principle from Vegetal Material. Romanian International Conference on Chemistry and Chemical Engineering, 12, 1-6
Departemen Pertanian, 2012, Peraturan Menteri Pertanian No 50 Tahun 2012 Tentang Pedoman Pengembangan Kawasan Pertanian, Jakarta.
Farhat, A., Fabiano-Tixier, A-S., Maataoui, M. E., Maingonnat, J-F.,Romdhane, M. Chemat, F. 2011.Microwave steam diffusion for extraction of essential oil from orange peel: Kinetic data, extract’s global yield and mechanism. Food Chemistry. 125/1: 255–261.
Ferhat M. A, Meklati B, Smadja J., Chemat F, (2006). An Improved Microwave Clevenger Apparatus For Distillation Of Essential Oils From Orange Peel. Journal of Chromatography A, Vol 1112, hal.121-126.
Fong, O. H. 2012. Extraction Of Essential Oil From Orange Peels.Thesis.Faculty of Chemical & Natural Resources Engineering, University Malaysia Pahang.
Golmakani M. dan Rezaei K., (2008).Comparison of microwave-assisted hydrodistillation with the traditional hydrodistillation method in the extraction of essential oils from Thymus vulgaris L. Food Chemistry, Vol. 109, hal. 925.
Hanif Z. dan Zamzami L., Balitjestro (2012).Trend Jeruk Impor dan Posisi Indonesia sebagai Produsen Jeruk Dunia. Badan Litbang Pertanian, Dirjend Hortikultura dan ACIAR. ISBN 978-979-8257-46-9.Hal.107-114.
Hermanto,S.2008. mengenal lebih jauh teknik Analisa Kromatografi dan spektrofotometri.Jakarta :Pusat Laboratorium Terpadu UIN Syarif Hidayatullah.
Hong-Wu Wang, Yan-Qing Liu, Shou-Lian Wei, Zi-jun Yan and Kuan Lu. 2010. Comparison of microwave-assisted and conventional hydro distillation in the extraction of essential oils from Mango (Mangifera indica L.). Flowers. Molecules, 15: 7715-7723; doi: 10.3390/molecules15117715
Kawana, S. Dan Miyagawa, H. 2011. Development of Green Technologies in GCMS-QP2010 Ultra Shimadzu Brochure, No.C146-E159. https://www.shimadzu.eu/default/Development-of-Green-Technologis-in-GCMS-QP2010-Ultra.pdf Diakes pada tanggal 20 maret 2014 pukul 11.35 WIB.
Megawati dan Murniyawati, F. 2015. Microwave Assisted Hydro-distillation untuk Ekstraksi Minyak Atsiri dari Kulit Jeruk Bali sebagai Lilin Aromaterapi. Jurnal Bahan Alam Terbarukan.4/1:18-26.
Pracaya. 1998. Bertanam Tomat. Kanisius, Yogyakarta
Saelarso, RB. 1996. Budidaya Jeruk Bebas Penyakit. Kanisius, Yogyakarta.
Sumeru, A. 2004. Biologi Reproduksi Tanaman Buah-buahan Komersial. Bayu Media Pub. Malang
Sawamura, M. (2010). Citrus Essential Oils: Flavor and fragrance. John Wiley & Sons, Inc., Publication. New Jersey.
Skoog, D.A., Holler, P. J., & Nieman, T.A. (2004). Principles of Instrumental Analysis Fifth Edition. Philadelpia: Hartcaurt Brace.
Suhirman, Shinta, Aplikasi Teknologi Pemurnian untuk Meningkatkan Mutu Minyak Nilam. Balai Penelitian Tanaman Obatdan Aromatik. Bogor (2009).
Sulaswatty, A., Wuryaningsih, dan Hartati, S. N. 2003.Pemurnian minyak Nilam (Pogostemon Cablin Benth) Menggunakan Teknik Ekstraksi Superkritis. Lembaga Ilmu Pengetahuan Indonesia.
Triana, A. W. 2013. Ekstraksi Minyak Atsiri Biji Kemukus dengan Metode Microwave Assisted Hydrodistillation. Semarang: Fakultas Teknik.
Wang, W. et al. 2010.Comparison of Microwave Assisted and Conventional Hydrodistillation in the Extraction of Essential Oils from Mango (Mangifera indica L.) Flowers. Molecules. 15:7715-7723.
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