VERIFIKASI METODE UJI TOTAL REDUCING SUGAR ICUMSA GS4/3-7 (2011)

Puji Pangestu Lestari, Zuhdi Ma'sum

Abstract


Based on ISO / IEC 17025: 2008 Clause 5.4 states that an accredited laboratory should select the appropriate method, already published in the international standard, regional or national, or reputable technical organizations or from the text or the relevant scientific journals. Laboratories should ensure that can operate standard methods before introducing the tests is to verify the standard method. As an accredited laboratory, the LP-P3GI need to perform verification testing methods to determine whether the total reducing sugar method ICUMSA GS4 / 3-7 (2011) can be applied or applied in LP-P3GI the results are valid and reliable, so that the results of the verification the method can be used as a quality assurance testing. In the verification method, a performance that will be tested is the precision (austerity). Precision is the degree of accuracy the value of some of the results of repeat testing. Precision test can be done by performing intra repeatability and reproducibility.
The results of precision test repeatability value CV = 0.75% < 2/3 CV Horwitz = 1.44%, while the intra-precision test reproducibility CV = 1.11%

Full Text:

PDF

References


Anonim.2011. Instruksi Kerja Validasi/ Verifikasi Metode. P3GI. Pasuruan.

Anonim.2011. Sesi I: Pengantar dan Filosofi Validasi Metode.BBIA. Bogor.

Anonim.2011. Sesi II: Perhitugan Statistik dalam Kimia Analisis. BBIA. Bogor.

Anonim.2011. Sesi III: Teknik dan Evaluasi Validasi Metode. BBIA. Bogor.

Anonim.2014. Sesi II: Perhitugan Statistik dalam Kimia Analisis. BBIA. Bogor.

Anonim.2014. Sesi II: Perhitugan Statistik dalam Kimia Analisis. BBIA. Bogor.

ICUMSA Method GS4/3-7.2011. The Determination of Total Reducing Sugars in Molasses and rafined Syrups after Hydrolysis by the Lane & Eynon Constant Volume Procedure- Official.

Panitia PK 03-01 Lembaga Penilaian Kesesuaian. 2008. Persyaratan Umum Kompetensi Laboratorium Pegujian dan Laboratorium Kalibrasi ISO/IEC 17025:2005, IDT. Depok

Santoso, BE, dkk. Pajalah Penelitian Gula. Penentuan Kadar Glukosaa dan Fruktosa dalam Tetes Tebu Menggunakan Metode Gabungan Polarisasi Ganda, Lane 7 Eynon dan Persamaan Standar Gula. P3GI. Pasuruan.

Sari, Rika.A. 2011. Validation Methode Practice. BBIA. Bogor.


Refbacks

  • There are currently no refbacks.


Copyright (c) 2017 eUREKA



eUREKA : Jurnal Penelitian Teknik Sipil dan Teknik Kimia

ISSN 2548-771X (online)

Email : [email protected]

 

Editorial Office :
Fakultas Teknik, Universitas Tribhuwana Tunggadewi Malang

Jl. Telaga Warna Blok C, Tlogomas, MALANG 65144, Jawa Timur
Tel / fax : (0341) 565 500 / (0341) 565 522

 

Creative Commons License
This work is licensed under a Creative Commons Attribution-ShareAlike 4.0 International License

 

View My Stats